Talk:MDMA Synthesis
| MDMA Synthesis | |||||||||||||||||||||||||||||||||
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| Chemical Nomenclature | |||||||||||||||||||||||||||||||||
| Common names | MDMA, Molly, Mandy, Emma, MD, Ecstasy, E, X, XTC, Rolls, Beans, Pingers | ||||||||||||||||||||||||||||||||
| Substitutive name | 3,4-Methylenedioxy-N-methylamphetamine | ||||||||||||||||||||||||||||||||
| Systematic name | (RS)-1-(Benzo[d][1,3]dioxol-5-yl)-N-methylpropan-2-amine | ||||||||||||||||||||||||||||||||
| Class Membership | |||||||||||||||||||||||||||||||||
| Psychoactive class | Stimulant / Entactogen | ||||||||||||||||||||||||||||||||
| Chemical class | Amphetamine / MDxx | ||||||||||||||||||||||||||||||||
| Routes of Administration | |||||||||||||||||||||||||||||||||
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This guide is provided for informational and educational purposes only. We do not encourage you to break the law and cannot claim any responsibility for your actions. |
This synth requires a basic understanding of Organic Chemistry (Instructions include How-To use the lab equipment required) and access to a few somewhat difficult to obtain materials. This synth makes 15g of pure MDMA Crystals.
Lab Equipment
- 24/40 500mL Round Bottom Flask, Ground Glass Joints
- 24/40 1000mL Round Bottom Flask, Ground Glass Joints
- 24/40 250mL Round Bottom Flask, Ground Glass Joints
- 24/40 Condenser, Ground Glass Joints
- 24/40 Distillation Adapter, Ground Glass Joints
- 24/40 Vacuum Adapter, Ground Glass Joints
- 24/40 Thermometer Adapter, Ground Glass Joints
- 0-300C Laboratory Thermometer
- 24/40 3-Way Adapter
- 3 Ten Inch Chemistry Stands
- Digital Hotplate/Magnetic Stirrer
- Teflon Coated Magnetic Stir Bar
- Glass Water Aspirator
- Boiling Stones
- 10 ft Vaccum Tubing
- Vaseline
- Pyrex 100ml Beaker
- 10 Quart Mason Jars
- Three Beam Analytical Balance
- Ph Pen
- Ax
- Sharp Knife
- Colander
- 1qt Steel Pot
- Funnel
- Cheesecloth
- Turkey Baster
- 3 Extention Clamps
- Clamp Fastener
Chemicals and Reagants
Buy more than listed, that way mistakes can be easily fixed!
Some measurements listed here are slightly overshot for this very reason
- Tide Detergent
- Lots of Water (Boiled)
- Lots of Sassafras Root Bark(See Preparation)
- 350ml Dimethylformamide
- 120g p-Benzoquinone
- 2g Palladium Chloride
- 5oom Methylene Chloride
- 1g HgCl2 Salt
- 5l Everclear
- 10ml Magnesium Sulphate
- Dry Pan
- 31.45% Muriatic Acid HCL
- 100% NaOH
- 500g Ammonium Chloride
- 500g Paraformaldehyde
- Peanut Oil
- 500ml
- 500ml Xylene
Synth
Lab Setup
- First off, make sure your lab has access to running water for the aspirator to make use of, water runs through it to create a vacuum inside of the distillation apparatus.
- Start by arranging your stands beside one another, then Place your clamps at a decent height, enough for an oil bath to fit under your flask.
- Clamp your 500ml Round Bottom Flask to the left stand around the neck of the Flask.
- Grease the tops of the joints of the Flask and the 3-way adapter and connect. then twist.
How to grease joints: Media:DistillGrease.jpeg
Diagram of 3-way adapter being connected: Media:3WayAdapterDistill.jpeg
- Grease the connections between the adaptor and the Condenser, then connect and twist. Secure condenser with clamp and stand.
Diagram of condencer being connected: Media:CondencerDistill.jpeg
- Grease and connect the Vaccum adapter, then the 250ml Round Bottom Flask.
- Ensure everything is tight and add clamps to ensure nothing moves.
What your setup should look like: Media:VaccumDistill.jpeg
- Now you know how to put the Pieces together, you will need to occasionally add and remove or swap parts out, this will be explained further as we go along.
Preparation
- Before starting I recommend cleaning everything with Tide detergent and warm water, making sure you have pre-measured everything, and make sure you have PLENTY of time to complete. A weekend should be ideal.
- WORK IN PROGRESS, more steps will be added later this week, taking a break for the time being. :))